The present invention provides methods, kits and compositions that are nontoxic color changing cleansers The cleansers include a mixture having a first component mixture and a second component mixture, wherein the first component mixture comprises a nontoxic color changing dye and the first component mixture in combination with the second component mixture such that the color of the nontoxic color changing dye is of a different color than the nontoxic color changing dye in the first component mixture. COLOR-CHANGING CLEANSING COMPOSITIONS AND METHODSFIELD OF THE INVENTIONThe invention generally relates to a cleansing composition. This invention also includes a method and kit for cleansing materials.
More particularly, the invention is directed to producing color changing soaps to facilitate promotion of hygiene and proper cleansing.BACKGROUND OF THE INVENTIONIt is often desirable to provide household toiletries such as soaps, shampoos with pleasant colors. Such colors are provided to household toiletries using dyes and pigments. Color-change has been a fascination of individual for long time. Traditionally, compounds that exhibited the ability for color change are leuco dyes.
Leuco dyes are of limited use to produce materials that begin as colored and end as colorless since three components are generally required to effect the transition. Generally, a color former (the leuco dye), a developer (such as phenolic compound) and a reversible matrix, such as long chain alcohol, are combined. An often noted drawback with leuco dye systems is their water insolubility.
Other limitations of leuco dye systems are commercial availability of all the colors and the cost.Approaches ensuring effective hand cleansing include antibacterial hand rubs. One drawback with such hand rubs is that such rubs may dry hands more than washing with soaps. Another approach known involves applying a dye that glows under a black light to hands prior to washing hands followed by washing hands and then analyzing the effectiveness of hand- washing process by examining the hands under a black light. In addition, some hospitals use electronic devices that alert an employee, if the employee's hands were not effectively washed.
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Building description. This 40 feet x 60 feet steel building has an eave height of 14 feet and 2400 sq. Of unobstructed interior space. The open layout of a rigid frame clear span offers the utmost adaptability at an economical price. All MBMI buildings are manufactured upon order. This is not a special to get rid of overstocked buildings.
Such approaches may be expensive and fail to achieve widespread use.SUMMARY OF THE INVENTION In view of the deficiencies of the prior art, it would be highly desirable to provide a color- changing cleansing composition, method and kit using nontoxic, non-staining colorants which provides an effective cleansing. Therefore, there is a need for an effective way of cleansing the hands while providing an indication that the cleansing is easy, effective, safe and inexpensive. The current invention provides such a composition, method and kit. There remains a need for a soap product that will give an indication of when sufficient use has occurred.
It is an object of this invention to provide such a use indicating soap. Conventional soaps used for hand washing do not indicate whether the soap has been used for an appropriate amount of time for the process to be effective. As a result, hands are often washed for too short an amount of time for the process to be effective in cleansing hands. Properly washing your hands is one of the best ways to prevent infection and the spread of diseases. Doctors, nurses andother people who work in medical settings have to wash their hands frequently to avoid spreading of infective agents.
Those who prepare food must keep clean hands so they do not put germs into the food they are making. Children and many adults do not always take the appropriate time needed to effectively clean their hands.
It is, therefore, quite important for children and adults to spend adequate time cleaning hands and learn the correct way of completing a key hygiene task. In order for proper hand cleaning habits to form, the teaching and monitoring must be done in a non-threatening and natural manner.
One way of accomplishing this would be introduce an element of fun and novelty so that children and adults enjoy completing the task while building better hygiene habits. Another way would be to give them a sense of accomplishment by providing a feedback signal they can easily understand and associate with correctly completing the task.Separate from the interest in removing microbes from the hands for hygiene, the greater scope of the effects of antimicrobial agents upon the environment and its effects upon bacterial resistance provide a driving force through which to accomplish the former, while minimizing the latter.
The object of this invention further provides a method through which proper hygiene is achieved by thorough washing for a minimum of 20 seconds using surfactants. It has been noted by 'Short- And Long-Term Effects Of Handwashing With Antimicrobial Or Plain Soap In The Community' Journal of Community Health,' Vol. 2, April 2003, sufficient hygiene can be achieved without the use of antimicrobial agents such as triclosan or quaternary ammonium salts. The invention provides color changing formulations containing both antimicrobial agents and without. Through the use of a color changing agent that works over a repeatable time window, the user confidently can use these formulations to achieve proper sanitation, without antimicrobials. The formulation without antimicrobials impact the environment by decreasing the load of antibacterial agents released into water supplies and contributing to the problem of microbial resistance.
'Strange but True: Antibacterial Products May Do More Harm Than Good,' Scientific American (June 7, 2007).The present invention fulfills the above-stated objective and overcomes these problems by broadly providing color-changing soap compositions, methods and kits that can encourage proper hand washing as a way to promote good hygiene. The inventors have developed novel color-changing soap composition for various cleansing applications.
It is therefore a principle object of the present invention to provide color-changing hand soap composition for effective cleansing. It is also an object of the present invention to provide novel color-changing composition, method and kit. It is a further object of the present invention to develop a new cleansing aid that provides a color-change detectible by a user after a period of time of rubbinghands together. The observable color-change may occur for a finite time, e.g., from 10 seconds to 5 minutes, or more particularly 10 to 45 seconds, or still more particularly between 25 to 35 seconds.
It is an additional object of the present invention to provide a composition that changes color during use includes natural colorants, synthetic colorants, acid-base indicators, FD&C dyes, D&C dyes. In one embodiment, flavin, phthalein or sulfonephthalein or azo compounds may be used as pH indicator. It is a further object of the invention to provide functionalized thickening agents that provide improved performance (i.e., color change) and improve the safety profile of a dye through linking to a polymer. The safety profile of polymers is known in the art, for example see EPA exemptions for polymers and co-polymers over 1OkD - www.epa.gov/EPA-PEST/2002/May/Day-24/pl2974.htm.The method through which a given dye changes its color is provided for with the following embodiments:1) A color changing hand soap that changes its color due to an decrease in pH brought about by the interaction with atmospheric carbon dioxide with the dye.
2) A surfactant composition interacting with the dye such that the surfactants control the rate through which the color changes.3) A surfactant mixture that forms supramolecular complexes with dyes, such as a micelle which controls the rate through which the absorbance of the dye changes.Absorbance is a physical quantity defined by Absorbance (A)= -logio Transmitance (T) = log Incident Radiant Power (Po)/Transmitted Radiant Power (P)To the end user, the change in absorbance is observed and a change in the color visible to the human eye. Ri = alkyl, benzylR 2 = alkyl, benzylR 3 = alkyl, benzylR 4 = alkyl group having C 6 to C 2o;X = anion include, but not limited to, halogen, sulfate, methosulfate, ethosulfate, sulfonate or carboxylate, acetate, nitrate, phosphate, saccharinate or tosylate.Other quaternary ammonium compounds and amine salts of the above general formula in the form of ring structures formed by covalently linking two of the radicals which may include heteroatom. Examples of such quaternary ammonium compounds and amine salts include, but are not limited to, imidazolines, imidazoliniums, pyridiniums, 2-heptadecyl-4,5-dihydro-lH- imidazol- 1 -ethanol, 4,5-dihydro- 1 -(2-hydroxyethyl)-2-isoheptadecyl- 1 -phenylmethyl- imidazolium chloride, 1 -2-oxo-2-2-(l -oxoctadecyl)oxyethylaminoethyl-pyridinium chloride.Other cationic surfactants include those compounds commonly referred to as 'ester quats', and as disclosed in US Patent 5,939,059, which is incorporated herein by reference. Typically, such materials are of general formula. Wherein X = an anion;R 1, R 2, R3 = same or different, straight or branched chain alkyl group from about C 2 to about Cs,'R 4 = saturated or unsaturated, straight or branched chain alkyl group from about Ci to about Cio, optionally substituted with halogen, hydroxyl, epoxy;Y 1, Y 2, Y3 = same or different, H, OH, aliphatic ester having saturated or unsaturated, straight or branched chain alkyl group from about C 10 to about C 25.
Further, cationic surfactants can also be antimicrobial compounds of the formula. WhereinR = alkyl or alkenyl group having from about C5 to about C 22; Ri = hydrogen or carboxyalkyl group having from about C 2 to about C 5;R 2 = hydroxyalkyl group having from about C 2 to about C 5; x = an integer from about 2 to about 8.Amidoalkyl betaines of the formula: O R 2R C Il H N (CH 2)X N I- + (CH 2)y CO 2R i;whereinR = alkyl or alkenyl group having from about C 5 to about C 22; R 1, R 2 = alkyl or hydroxyalkyl group having from about Ci to about C5; x = an integer from about 2 to about 8.Phosphobetaines of the formula. WhereinR = alkyl or alkenyl group having from about C 5 to about C 22; Ri = alkylene or hydroxy alky lene group having from about C 2 to about C5;R 2 = hydrogen or carboxyalkyl group having from about C 2 to about C 5;R 3 = hydroxyalkyl group having from about C 2 to about C 5; x = an integer from about 2 to about 8.In one embodiment, the phosphobetaine compounds are those disclosed in US Patents 4215064, 4617414, 4233192, which are all incorporated herein by reference.Pyrophosphobetaines of the formula. The term 'FD&C' and 'D&C' dyes are recognized in the art. In the United States, colorants for food, drug and cosmetics are regarded as 'color additives'. The Federal Food, Drug & Cosmetic (FD&C) Act of 1938 made food color additives certification mandatory. Since then Food and Drug Administration (FDA) has been responsible for regulating all color additives used in food, drugs and cosmetics.
Each batch to be sold in the United States has to be certified by the FDA. To avoid confusing color additives used in food with those manufactured for other uses, three categories of certifiable color additives were created: 1) FD&C (Food, Drugs & Cosmetics) color additives with application in food, drugs & cosmetics; 2) D&C (Drugs & Cosmetics) color additives with application in drugs & cosmetics; 3) External D&C (External Drugs & Cosmetics) color additives with applications in externally applied drugs & in externally applied cosmetics. Lakes are colorants prepared by precipitating a soluble colorant onto an insoluble base or substratum. A variety of bases such as alumina, titanium dioxide, zinc oxide, talc, calcium carbonate and aluminum benzoate are approved for D&C colorants, while only alumina is permitted as the substrate for manufacturing FD&C lakes. The use of all food colors approved for use in the United States are listed in 21 C. (Code of Federal regulations), parts 70 through 82 dealing with color additives.Representative examples of FD&C dyes, D&C dyes, Ext.
D&C dyes for use with the present invention include, but are not limited to, FD&C Blue 1, FD&C Blue 2, FD&C Green 3, FD&C Red 3, FD&C Red 4, FD&C Red 40, FD&C Yellow 5, FD&C Yellow 6, Citrus Red 2, Orange B, D&C Blue 4, D&C Blue 6, D&C Blue 9, D&C Brown 1, D&C Green 5, D&C Green 6, D&C Green 8, D&C Orange 4, D&C Orange 5, D&C Orange 10, D&C Orange 11, D&C Red 6, D&C Red 7, D&C Red 17, D&C Red 21, D&C Red 22, D&C Red 27, D&C Red 28, D&C Red 30, D&C Red 31, D&C Red 33, D&C Red 34, D&C Red 36, D&C Red 39, D&C Violet 2, D&CYellow 7, D&C Yellow 8, D&C Yellow 10, D&C Yellow 11, Ext. D&C Violet 2, Ext. WhereinR 2, R 3, R 5, R 6, R 7, R 8, R 9 Rio = H, OH, Cl, Br, I, OR', CN, NO 2, NH 2, NHR', NR'R', NHCOR', SH, SO 3H, SO 3M, COOH, COOM, alkyl, alkoxy, aryl, cycloalkyl, hetaryl R' = alkylR' = alkylM = metalRepresentative examples of tripheylmethane acid-base indicators of the present invention include, but are not limited to, acid fuchsin, alkali blue, aurin, crystal violet, ethyl violet, heptamethoxy red, hexamethoxy red, malachite green, methyl green, methyl violet, patent blue V, pentamethoxy red, poirrier blue C 4B, p-rosolic acid, rubrophen and mixtures thereof. Representative examples of miscellaneous acid-base indicators of the present invention include, but are not limited to, curcumin, hematoxylin, indigo carmine, indophenol, isonitrosothiocamphor, neutral red, phenolmalein, resazurin, alizarin red, alizarin red S, pinachrome, quinaldine red, quinoline blue, anilinesulfonephthalein, benzoflavine, bromopyrogallol red, lacmoid, methyl purple, oxine blue, tobias acid and mixtures thereof.
Additionally, substituted hydrazides based acid-base indicators are useful herein, as given by the general formula. The edible pH indicator includes any substance that changes color in response to the pH of the solution it is dissolved in.
Edible indicators are non-toxic when consumed in amounts that are effective for detecting color changes due to pH variations. The pH indicator may be responsive to narrow or broad pH ranges, and may be show the greatest colorimetric response at alkaline pH ranges, acidic pH ranges, or neutral pH ranges.
Particularly useful pH indicators for use in the instant beverage composition include anthocyanins. Anthocyanins are typically present in extracts of red cabbage, such as red cabbage juice, or red cabbage powder. Such extracts of red cabbage are a particularly useful edible pH indicator for inclusion in the first mixture. Red cabbage extracts are typically blue or green at high pH levels (more basic) purple at neutral pH levels, and pink to red at low pH levels (more acidic). In addition, the present invention may also include coloring agents may include any of a variety of natural or artificial food colorings that are non-toxic and known in the art, including Red no. 2 (amaranth), Red no. 3 (erythrosine), Red no.
4 (Ponceau SX), DC Red no. 22 (eosine), Red no. 28 (phloxine), Red no. 40 (Allura Red; or disodium salt of 6-hydroxy-5(2-methoxy-5-methyl-4- sulfop- henyl) azo-2-naphthalenesulfonic acid), Yellow no. 5 (tartrazine; trisodium 5-hydroxy- l-(4-sulfonatophenyl) (4-sulfonatophenylazo)-H-pyrazo- le-3-carboxylate), DC Yellow no.
1 (quinoline yellow SS), Yellow no. 6 (Sunset Yellow FCF; or disodium salt of 6-hydroxy-5-(4- sulfophenyl)azo 2-naphthalenesulfonic acid)), DC Yellow no. 10 (Quinoline Yellow WS), Green no.
3 (Fast Green FCF), DC Green no. 5 (Alizarine Cyanine Green F), DC Green no. 6 (Quinizarine Green SS), Blue no.
1 (Brilliant Blue FCF), Blue no. 2 (Indigo Carmine), annatto, anthocyanins, beet extracts, beta-carotene, caramel, carmine/cochineal, paprika oleoresin, andturmeric, among others. In one embodiment of the invention, the coloring agents include one or more of anthocyanins, and Yellow no.
5.EXAMPLE 1Stepanol ABHS-15C 2O g o-Cresolphthalein 0.5 gSodium hydroxide 0.11 gDI water 77.79 gSodium chloride 1.5 gPreservative 0.1 g A mixture of Stepanol ABHS- 15C, fragrance and DI water was stirred until homogeneous, o-Cresolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 2 Stepanol DCFAS-F/N 3.5 gNinol 40CO 1 g o-Cresolphthalein 0.5 gSodium hydroxide 0.11 gDI water 93.29 g Sodium chloride 1.5 gPreservative 0.1 gA mixture of Stepanol DCFAS-F/N in DI water was stirred until completely dissolved and homogeneous followed by addition of Ninol 40CO. O-Cresolphthalein was added to the mixture followed by addition of sodium hydroxide.
The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 3Bio-Terge AS-40 15.4 gSteol CS-460 9 gAmphosol CA 4 g Ninol 40-CO 1 gThymolphthalein 0.5 gSodium hydroxide 0.09 gDI water 68.41 gSodium chloride 1.5 g Preservative 0.1 gA mixture of Bio-Terge AS-40 in DI water was stirred until homogeneous followed by addition of Steol CS-460, Amphosol CA and Ninol 40-CO.
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Thymolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight). EXAMPLE 4Bio-Terge AS-40 15.4 gSteol CS-460 9 gAmphosol CA 4 gNinol 40-CO 1 go-Cresolphthalein 0.5 gSodium hydroxide 0.11 gDI water 68.49 gSodium chloride 1.5 g Preservative 0.1 gA mixture of Bio-Terge AS-40 in DI water was stirred until homogeneous followed by addition of Steol CS-460, Amphosol CA and Ninol 40-CO.
O-Cresolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight). EXAMPLE 5Amphosol HCA 4 gSteol CS-330 1O gNinol 40-CO 0.5 g o-Cresolphthalein 0.5 g Sodium hydroxide 0.11 gDI water 83.29 gSodium chloride 1.5 gPreservative 0.1 g A mixture of Amphosol HCA in DI water was stirred until homogeneous followed by addition of Steol CS-330 and Ninol 40-CO.
O-Cresolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 6Cola Terric SLAA 42.8 g Colamid ALCola Lipid C 2 gThymolphthalein 0.5 gSodium hydroxide 0.09 gDI water 53.01 g Sodium chloride 1.5 gPreservative 0.1 gA mixture of Cola Terric SLAA, Cola Lipid C and DI water was stirred until homogeneous.Thymolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 7Colonial SLS 20.00 gColamid AL 0.5 g o-Cresolphthalein 0.5 g Sodium hydroxide 0.11 gDI water 77.29 gSodium chloride 1.5 gPreservative 0.1 gA mixture of Colonial SLS, Colamid AL in DI water was stirred until homogeneous, o- Cresolphthalein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).
EXAMPLE 8Bio-Terge AS-40 15.4 gSteol CS-460 9 gAmphosol CA 4 gNinol 40-CO 1 g Fluorescein 0.2 gSodium hydroxide 0.05 gDI water 68.75 gSodium chloride 1.5 gPreservative 0.1 g A mixture of Bio-Terge AS-40 in DI water was stirred until homogeneous followed by addition of Steol CS-460, Amphosol CA and Ninol 40-CO. Fluorescein was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride.
Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 9 Colonial SLS 20.00 gColamid AL 0.5 gPeonidin HCl 0.010 gSodium hydroxide 0.11 gDI water 77.29 g Sodium chloride 1.5 gPreservative 0.1 gA mixture of Colonial SLS, Colamid AL in DI water was stirred until homogeneous.PeonidinΗCl was added to the mixture followed by addition of sodium hydroxide. The viscosity was adjusted by addition of sodium chloride. Preservative was added and the mixture was stirred for 2 hours (preferably overnight).EXAMPLE 10Colonial SLS 20.00 gColamid AL 0.5 gDye 0.100 g Sodium hydroxide 0.11 gDI water 77.29 gSodium chloride 1.5 gPreservative 0.1 g A mixture of Colonial SLS, Colamid AL in DI water was stirred until homogeneous. The dye one of the following D&C Red No 6, D&C Red No 33, D&C Orange No 4, FD&C Yellow No 5, FD&C Red No 40, Food Yellow 1, FD&C Yellow No 6 (Sunset Yellow FCF), Sudan III (D&C Red No 17), FD&C Blue no 2, Curcumin, D&C Yellow No 10, FD&C Green No 3, D&C blue no 4, Chrome Azurol S, D&C Blue No 4, FD&C Blue No 1, Food Blue 3, FD&C Green No1, was added to the mixture followed by addition of analyte one of the following: cupric acetate, zinc aceate, calcium acetate, magnesium acetate, sodium carbonate, or potassium carbonate. Preservative was added and the mixture was stirred for 2 hours (preferably overnight). EXAMPLE 11Colonial SLS 20.00 gColamid AL 0.5 gDye 0.100 gSodium hydroxide 0.11 g DI water 77.29 gSodium chloride 1.5 gPreservative 0.1 g A mixture of Colonial SLS, Colamid AL in DI water was stirred until homogeneous. A method of forming a nontoxic color changing cleanser composition comprising the steps: providing a cleanser mixture comprising a first component mixture and a second component mixture; and mixing the first component mixture and the second component mixture, wherein the first component mixture comprises a nontoxic color changing dye and the first component mixture in combination with the second component mixture such that the color of the nontoxic color changing dye is of a different color than the nontoxic color changing dye in the first component mixture.
A method of making a nontoxic color changing cleanser composition comprising making a cleanser mixture comprising: mixing separately a first component mixture and a second component mixture, wherein the first component mixture comprises a nontoxic color changing dye and the first component mixture in combination with the second component mixture such that the color of the nontoxic color changing dye is of a different color than the nontoxic color changing dye in the first component mixture, wherein upon contact between the first and second component the cleanser mixture changes color.
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